Prof. Dr. Siegfried R. Waldvogel - Elektrosynthese

Vita

Dipl.-Chem. Univ. (Chemie) University of Konstanz (1990-1994)
PhD University of Bochum / Max-Planck-Institut für Kohlenforschung (1994-1996)
Postdoc Scripps Research Institute in La Jolla, California; DAAD/NATO fellowship (1997-1998)
Habilitation University of Münster (2004)
Professor (C3/W2) University of Bonn (2004-2010)
Full Professor (W3) University of Mainz (seit 2010)
Direktor Elektrosynthese, MPI CEC (seit Nov. 2023)
   
Publications

Complete list of publications (.pdf) | Google Scholar | ORCID

Complete list of publications also on: AK Waldvogel | Johannes Gutenberg Universität Mainz

Recent Publications

2024

449.

B. Pavlovic, C. Heubel, M. Kurz, E. Oehl, S. Waldvogel, M. Méndez, S. Ruf, Single Steop Synthesis of β- γ-aryl-substituted β- and γ Amino Acid Derivatives by Electrochemistry, Bioorg. Med. Chem. Lett., 2024, [accepted].

448.

D. F. Nater, P. Hendriks, S. R. Waldvogel, Electrochemical Hofmann Rearrangement at High Current Densities in a Simple Flow Setup, Mol. Catal., 2024, [accepted].

447.

L. G. Gombos, J. Nikl, and S. R. Waldvogel, Dual Roles of Supporting Electrolytes in Organic Electrosynthesis, ChemElectroChem, 2024, [accepted].

446.

I. Dinges, I. Depentori, L. Gans, D. Holtmann, S. R. Waldvogel, and M. Stöckl, Coupling of CO2 Electrolysis with Parallel and Semi-Automated Biopolymer Synthesis – Ex-Cell and without Downstream Processing, ChemSusChem, 2024, [accepted].

2023

445.

S. R. Waldvogel, S. Arndt, R. Gross, Method for preparing periodates via anodic oxidation in a steady state reactor, 2023, WO2023194432 A1.

444.

S. R. Waldvogel, DUZ Wissenschaft & Management 2023, 10 (1. Dec.), 32.

443.

J. C. Bieniek, B. Mashtakov, D. Schollmeyer, S. R. Waldvogel, Dehydrogenative Electrochemical Synthesis of N-Aryl-3,4-Dihydroquinolin-2-ones by Iodine(III)-Mediated Coupling Reaction, Chem. Eur. J. 2023, e202303388. [DOI: 10.1002/chem.202303388]

442.

P. Moreno-García, M. J. Gálvez-Vázquez, T. Prenzel, J. Winter, L. Gálvez-Vázquez, P. Broekmann, S. R. Waldvogel, Self-standing Metal Foam Catalysts for Cathodic Electro-organic Synthesis, Adv. Mater. 2023, 2307461. [DOI: 10.1002/adma.202307461]

441.

J. Schneider, S. P. Blum, S. R. Waldvogel, Electrochemical Synthesis of Sulfonamides in Single-Pass Flow, ChemElectroChem 2023. [DOI: 10.1002/celc.202300456]

440.

F. Sprang, S. R. Waldvogel, J. Schuetz, W. Bonrath, R.  Goy, A process for producing benzoquinones, PCT Int. Appl. 2023, WO2023161206 A1.

439.

F. Weinelt, F.-E. Baumann, S. R. Waldvogel, S. Hofmann, J. Nikl, Electrochemical oxidation of cycloalkenes to form α, ω-dicarboxylic acids and ketocarboxylic acids, PCT Int. Appl. 2023, WO2023186658 A1.

438.

F. Weinelt, F.-E. Baumann, S. R. Waldvogel, A.-L. Rauen, J. Nikl, Electrochemical oxidation of cycloalkanes to form cycloalkanone compounds, PCT Int. Appl. 2023, WO2023186659 A1.

437.

F. Weinelt, F.-E. Baumann, S. R. Waldvogel, K. Hofman, J. Nikl, Electrochemical oxidation of fatty acids and fatty acid esters to form monocarboxylic acids and alpha-omega-dicarboxylic acids, PCT Int. Appl. 2023, WO2023186660 A1.

436.

F. Weinelt, F.-E. Baumann, S. R. Waldvogel, J. Nikl, Electrochemical oxidation of cycloalkenes and cycloalkanes into α,ω-dicarboxylic acids or into ketocarboxylic acids and cycloalkanone compounds, PCT Int. Appl. 2023, WO2023186661 A1.

435.

S. Hofmann, J. Winter, T. Prenzel, M. J. Gálvez-Vázquez, S. R. Waldvogel, Electrochemical Synthesis of Isoxazoles and Isoxazolines via Anodic Oxidation of Oximes, ChemElectroChem 2023, 10, e202300434. [DOI: 10.1002/celc.202300434]

434.

A. Schüll, L. Grothe, E. Rodrigo, T. Erhard and S. R. Waldvogel, Electrochemical Synthesis of S-Aryl Dibenzothiophenium Triflates as Precursors for Selective Nucleophilic Aromatic (Radio)-Fluorination, Org. Lett. 2023, [accepted]. [DOI: 10.1021/acs.orglett.3c02921]

433.

R. Siedentop, T. Prenzel, S. R. Waldvogel, K. Rosenthal and S. Lütz, Reaction Engineering and Comparison of Electroenzymatic and Enzymatic ATP Regeneration Systems, ChemElectroChem 2023, e202300332. [DOI: 10.1002/celc.202300332] (highlighted with front cover)

432.

M. Linden, S. Hofmann, F. N. Weber, R. M. Bär, S. J. Kaldas, M. J. Ford, and S. R. Waldvogel, From Screening to Hectogram Scale: Sustainable Electrochemical Synthesis of Mefenpyr-diethyl, Green Chem. 2023, [accepted]. [DOI: 10.1039/D3GC02118A]

431.

M. Klein, D. Troglauer, S. R. Waldvogel, Dehydrogenative Imination of Low-Valent Sulfur Compounds – Fast and Scalable Synthesis of Sulfilimines, Sulfinamidines, and Sulfinimidate Esters, Synform 2023, 55, A135–A136. [DOI: 10.1055/s-0040-1720603]

430.

J. Nikl, K. Hofman, S. Mossazghi, I. C. Möller, D. Mondeshki, F. Weinelt, F.-E. Baumann, S. R. Waldvogel, Electrochemical oxo-functionalization of cyclic alkanes and alkenes using nitrate and oxygen, Nat. Commun. 2023, 14, 4565. [DOI: 10.1038/s41467-023-40259-0] Highlited in Phys.org

429.

R. J.-R. Bednarz, P. Jiménez-Meneses, A. S. Gold, D. Monllor-Satoca, A. Stenglein, R. Gómez, S. R. Waldvogel, Sustainably scaled electrochemical synthesis of 3-propyladipicacid in line with fluctuating grid supply, ChemCatChem 2023, e202300606. [DOI: 10.1002/cctc.202300606]

428.

R. J.-R. Bednarz, A. S. Gold, J. Hammes, D. F. Rohrmann, S. Natalello, M. Mann, F. Weinelt, C. Brauer, S. R. Waldvogel, Scaled oxidative flow electrosynthesis of 3-alkyladipic acids from 4-alkylcyclohexanols, Org. Process Res. Dev. 2023. [DOI: 10.1021/acs.oprd.3c00146]

427.

O. Oseghe, F. Guba, A. Misra, R. Gong, R. Liu, S. R. Waldvogel, D. Ziegenbalg, C. Streb, D. Gao, A scalable flow device for the removal of organic and inorganic pollutants from water, Device, 2023, [accepted]

426.

M. M. Hielscher, M. Dörr, J. Schneider, S. R. Waldvogel, LABS: Laboratory Automation and Batch Scheduling – A Modular Open Source Python Program for the Control of Automated Electrochemical Synthesis with a Web Interface, Chem. Asian J. 2023, 18, e202300380. [DOI: 10.1002/asia.202300380]

425.

I. Waldvogel, S. R. Waldvogel, Elektrochemische Gewinnung - Vanillin aus Lignin als innovative, „grüne“ und nachhaltige Methode, Der Lebensmittelbrief 2023, 34, May-June, 42-43.

424.

S. Hofmann; M. Linden; J. Neuner; F. N. Weber; S. R. Waldvogel, Electrochemically Enabled Oxidative Aromatization of Pyrazolines, Org. Biomol. Chem. 2023, 4694–4701. [DOI: 10.1039/D3OB00671A]

423.

F. Sprang; J. Klein; S. R. Waldvogel, Direct Anodic Conversion of 4-Hydroxybenzaldehydes into Benzoquinones, ACS Sustain. Chem. Eng. 2023. [DOI: 10.1021/acssuschemeng.3c00257]

422.

C. Kisukuri; J. Seidler; D. Rohrmann; T. Gärtner; S. R. Waldvogel, Scalable Electrochemical Reduction of Nitrobenzotrifluorides to 3-Trifluoromethylanilines,  Org. Process Res. Dev. 2023.  [DOI: 10.1021/acs.oprd.3c00067]

421.

C. Stork, R. Weck, M. Valero, H. Kramp, S. Güssregen, S. R. Waldvogel, A. Sib, V. Derdau, Hydrogen Isotope Exchange by Homogeneous Iridium Catalysis in Aqueous Buffers with Deuterium or Tritium gas, Angew. Chem. Int. Ed. 2023, e202301512. [DOI: 10.1002/anie.202301512

420.

P. J. Kohlpaintner, L. Marquart, L. J. Gooßen, S. R. Waldvogel, The Oxidation of Organo-Boron Compounds Using Electrochemically Generated Peroxodicarbonate, Eur. J. Org. Chem. 2023, e202300220. [DOI: 10.1002/ejoc.202300220]

419.

O. Koleda, T. Prenzel, J. Winter, T. Hirohata, M. de Jesus Gálvez-Vázquez, D. Schollmeyer, S. Inagi, E. Suna, S. R. Waldvogel, Simple and Scalable Electrosynthesis of 1H-1-Hydroxy-quinazolin-4-ones, Chem. Sci. 2023, 14, 2669–2675. [DOI: 10.1039/D3SC00266G]

418.

M. Zirbes, T. Graßl, R. Neuber, S. R. Waldvogel, Peroxodicarbonate as a Green Oxidizer for the Selective Degradation of Kraft Lignin into Vanillin, Angew. Chem. Int. Ed. 2023, e202219217 published online 31.01.2023. [DOI: 10.1002/anie.202219217]M. Zirbes, T. Graßl, R. Neuber, S. R. Waldvogel, Peroxodicarbonate as a Green Oxidizer for the Selective Degradation of Kraft Lignin into Vanillin, Angew. Chem. 2023, e202219217 published online 31.01.2023. [DOI: 10.1002/ange.202219217]

417.

A. D. Beck, S. Haufe, S. R. Waldvogel, General Concepts and Recent Advances in the Electrochemical Transformation of Chloro- and Hydrosilanes, ChemElectroChem 2023, 10, e202201149. [DOI: 10.1002/celc.202201149] (Inside Cover)

416.

M. Klein, D. Troglauer, S. R. Waldvogel, Dehydrogenative Imination of Low-Valent Sulfur Compounds – Fast and Scalable Synthesis of Sulfilimines, Sulfinamidines, and Sulfinimidate esters, JACS Au 2023, 3, 2, 575–583. [DOI: 10.1021/jacsau.2c00663]

415.

J. Klein, S. R. Waldvogel, Selective Electrochemical Degradation of Lignosulfonate to Bio-Based Aldehydes, ChemSusChem 2023, e202202300 published online 18.01.2023. [DOI: 10.1002/cssc.202202300]

414.

S. B. Beil, S. R. Waldvogel, Trendberichte Organische Chemie - Rubrik "Elektrosynthese", Nachr. Chem. 2023, 71, 41–42. [DOI: 10.1002/nadc.20234135542]

413.

J. Klein, R. Kupec, M. Stöckl, S. R. Waldvogel, Degradation of Lignosulfonate to Vanillic Acid Using FerrateAdv. Sustainable Syst. 2022, 2200431 published online 25.12.2022. [DOI: 10.1002/adsu.202200431]

412.

J. Seidler, A. Roth, L. Vieira, S. R. Waldvogel, Electrochemical CO2 utilization for the synthesis of α-hydroxy acids, ACS Sustain.Chem.Eng. 2023, 11, 390–398. [DOI: 10.1021/acssuschemeng.2c06046]

411.

M. Linden, S. Hofmann,  A. Herman, N. Ehler, R. M. Bär, S. R. Waldvogel, Electrochemical Synthesis of Pyrazolines and Pyrazoles via [3+2] Dipolar Cycloaddition, Angew. Chem. Int. Ed. 2023, 62, e202214820. [DOI: 10.1002/anie.202214820] M. Linden, S. Hofmann,  A. Herman, N. Ehler, R. M. Bär, S. R. Waldvogel, Electrochemical Synthesis of Pyrazolines and Pyrazoles via [3+2] Dipolar Cycloaddition, Angew. Chem. 2023, 135, e202214820. [DOI: 10.1002/ange.202214820]

410.

J. Winter, T. Prenzel, T. Wirtanen, D. Schollmeyer, S. R. Waldvogel, Direct Electrochemical Synthesis of 2,3-Disubstituted Quinoline N-oxides by Cathodic Reduction of Nitro Arenes, Chem. Eur. J. 2023, 29, e202203319. [DOI: 10.1002/chem.202203319]

409.

A. D. Beck, L. Schäffer, S. Haufe, S. R. Waldvogel, Assessment of the Electrochemical Synthesis Route to Silicones Starting from Silica as Feedstock, Eur. J. Org. Chem. 2022, e202201253. [DOI: 10.1002/ejoc.202201253]

408.

X. Dong, M. Klein, S. R. Waldvogel, B. Morandi Controlling Selectivity in Shuttle Hetero-difunctionalization Reactions: Electrochemical Transfer Halo-thiolation of Alkynes, Angew. Chem. Int. Ed. 2023, 62, e202213630. [DOI: 10.1002/anie.202217110]
X. Dong, M. Klein, S. R. Waldvogel, B. Morandi Controlling Selectivity in Shuttle Hetero-difunctionalization Reactions: Electrochemical Transfer Halo-thiolation of Alkynes, Angew. Chem. 2023, 135, e202213630. [DOI: 10.1002/ange.202217110]

Preise, Ehrungen & Auszeichnungen

1996 Otto-Hahn-Medal of the Max-Planck-Society
2001 Bennigsen-Foerder-Award of the state of North Rhine Westphalia
2001 Donation by the Dr.-Otto-Röhm-Foundation
2003 Young researchers award by the “Förderkreis der Westfälischen Wilhelms-Universität”
2003 Fellowship by the Hellmut Bredereck-Foundation (GDCh)
2008 Inventors Award "Patente Erfinder" of the state of North Rhine Westphalia, 2nd award
2008 Nicolas-August-Otto-Award of the city of Cologne, 2nd award
2013 Zukunftspreis Pfalz
2018 Jaroslav Heyrovsky Prize for Molecular Electrochemistry (International Society of Electrochemistry)
2019/2020 Novartis Chemistry Lecture Award
2020 Manuel M. Baizer Award (Electrochemical Society)
2020 Pitch of the year (CHEManager) with ESy-Labs GmbH
2022 Sigma-Aldrich Lecture (Merck)
2023 UNIPRENEURS Award (German Federal Ministry of Education and Research and the German Federal Ministry of Economics and Climate Protection)
Abteilungsmitglieder

Projektkoordination

Dr. Simon Trosien

Postdocs

Dr. Tomas Horsten
Dr. Darryl Frédéric Nater
Dr. Tim Pieter van Lingen

PhD Studierende

Malte Deters
Finn Moeller
Aaron Schüll
Niclas Schupp

Labor

Maximilian Conradt
Norbert Dickmann
Nina Dotzauer
Tobias Stamm

Forschungsprofil 'Elektrosynthese'

News on SFB 1633 (CRC 1633 - Pushing Electrons with Protons)